Table 10

X-ray structural analysis of the phase composition of the surface layer of high-speed steel of the gear-shaping cutters after nitriding at different gas ratios at nitriding temperature of 480 °С and holding time of 45 min.

Phase composition Volume fraction of phase (%) in nitrided layer

  20% N2 + 80% Ar 40% N2 + 60% Ar 60% N2 + 40% Ar
Radiation used: CuKa (shooting in sliding geometry)
Fe2N 7.5 19.9
Mo2N 20.8 18.7 14.3
Fe3(W,Mo)3(C,N) 34.6 32.3 26.2
Feα(C,N) 44.6 41.5 39.6
Radiation used: CuKa
Fe2N 4.1
Mo2N 5.2 7.8 8.2
Fe3(W,Mo)3(C,N) 5.7 11.9 12.0
Feα(C,N) 89.1 80.3 75.7

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